Cure and Aging Monitoring of Epoxies by Fluorescence Spectroscopy
Demonstrated intrinsic fluorescence of resin.
Found one-to-one correspondence of fluorescence intensity ratio with conversion (0-100%) allowing for robust cure monitoring.
Physical aging of fully-cured resin may be monitored with fluorescence intensity ratio.
Demonstrated feasibility of cure monitoring via fiber-optic based fluorescence using commerical instrumentation.

Fiber-optic Monitoring Equipment


Fiber-optic Ultrasound Sensors for Process Monitoring

Objectvie:
Integrate fiber-optic ultrasound cure monitoring system with RTM. Such a system can be used at higher temperaturee than pzt-based systems.
Accomplishments: Distributed broadband Sagnac ultrasound sensor with enhanced sensitivity designed and characterized.
First prototype of a local Bragg-grating ultrasound sensor devised.
Fiber-optic Ultrasound Generators devised.
Sagnac sensor embedded into a composite ply and tested in the presence of high temperature and pressure that prevail inside an RTM setup.
A new instrumented model has been designed and constructed. This mold contains ports for bringing the Sagnac sensor into the mold cavity. The top half of the mold also contains a new system for fiber-optic ultrasound generation.
Preliminary results for cure monitoring using the above instrumented RTM setup have been obtained.

Integration of Laser Based Ultrasound System in RTM Environment

Cure monitoring with Fiberoptic Ultrasonic sensors

Cure Monitoring


MEASURE
at different times during cure:

  • ultrasonic wavespeed from time of flight measurements
  • ultrasonic attenuation from amplitude measurements

INFER:

  • gel point
  • glass transition temperature
  • degree of cure
  • porosity of cured component

ADVANTAGE: monitor cure at any selected layer rather than get a through-thickness average measurement



Home | Mission | Participants | Overview | Projects | People | Links